High energy ball milling was investigated as a technique to achieve the exfoliation of clay minerals Delamination of the Na montmorillonite particles was observed after 3 h of ball milling at 40 rpm 20 to 1 balltopowder ratio and after 1 h of milling at 400 rpm 5 to 1 balltopowder ratio For organomontmorillonite Cloisite 30B the separation of the clay mineral layers could not be achieved by 3 h of
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